The CCIC NMR facility underwent major renovations in 2014-2015, expanding our capabilities with nine high-field instruments. Our current setup includes five solution, two solid-state NMR systems including DNP, and two mixed use instruments across two campus locations.
Instruments
Explore Ohio State's leading-edge NMR capabilities.
Riffe 137 / 496 W 12th Ave
- Software: TopSpin 3.6.2 running on CentOS 7
- Probe: 5mm Triple-resonance Inverse (TXI) cryoprobe with Z-Gradients
- Features: Automatic Tuning/Matching, Temperature controlled SampleJet (up to 510 samples), High-sensitivity 1H, Bluefors helium reliquefier
- Location: Riffe 137
- Software: TopSpin 3.7 running on CentOS 7
- Probe: 5mm Triple-resonance Observe (TXO) cryoprobe with Z-Gradients
- Features: Automatic Tuning/Matching, Temperature controlled SampleJet (up to 510 samples), Nitrogen Liquefier, High-sensitivity 1H, 13C, & 15N
- Location: Riffe 137
- Software: TopSpin 3.7 running on CentOS 7
- Probe: 5mm Quadrupole-resonance Inverse (QCI-P) cryoprobe with Z-Gradients
- Features: SampleCase (up to 24 samples), Nitrogen Liquefier, High-sensitivity 1H and 13C, plus dedicated 15N and 31P channels
- Location: Riffe 137
CBEC 092 / 151 W Woodruff Ave
- Software: TopSpin 3.7 running on Windows 10
- Probe: 5mm Broadband Observe solution iProbe with Z-Gradients (29Si to 19F)
- Features: SampleCase (up to 24 samples), Automatic Tuning/Matching, Liquid Nitrogen VT capability
- Location: CBEC 092
- Software: TopSpin 3.7 running on CentOS 7
- Probes:
- 3.2mm HXY LTMAS for DNP
- 3.2mm HCN LTMAS for DNP
- 1.3mm HCN very-fast MAS solid-state probe
- Features: Bruker Biospin 395 GHz Gryotron System with LT-MAS cooling unit
- Location: CBEC 092
- Software: TopSpin 4.4.1 running on CentOS 7
- Probes:
- 5mm Quadruple-resonance Inverse solution probe (QXI-F) with (1H, 13C, 15N, 19F, 2H)
- 5mm Triple-resonance Inverse solution probe (TXI) with (1H, 13C, 15N, 2H)
- 4.0mm Gradient hr-MAS solid-state probe (1H, 13C, 15N, 2D)
- 3.2mm Efree solid-state probe (1H, 13C, 15N, 2H)
- 2.5mm Tri-gamma solid-state probe (15N to 31P, and 1H)
- 1.9mm Very-fast MAS solid-state probe (1H, 13C, 15N)
- 1.3mm Very-fast MAS solid-state probe (1H, 13C, 15N)
- 0.7mm Ultra-fast MAS solid-state probe (1H, 13C, 15N)
- Features: SampleCase, Liquid Nitrogen VT capability
- Location: CBEC 092
- Software: TopSpin 3.7 running on CentOS 7
- Probes:
- 3.2mm Efree solid-state probe (1H, 13C, 15N, 2H)
- 1.9mm Very-fast MAS solid-state probe (1H, 13C, 15N)
- 1.3mm Very-fast MAS solid-state probe (1H, 13C, 15N)
- 0.7mm Ultra-fast MAS solid-state probe (1H, 13C, 15N)
- 3.2mm HXY solid-state probe
- Features: Helium Liquefication for near-zero instrument maintenance
- Location: CBEC 092
- Software: TopSpin 3.7 running on CentOS 7
- Probe: 5mm Triple-resonance Inverse (TCI) cryoprobe with Z-Gradients
- Features: Temperature controlled SampleCase (up to 24 samples), Nitrogen Liquefier, Dual-Receiver, High-sensitivity 1H & 13C
- Location: CBEC 092
- Software: TopSpin 4.4.1 on CentOS 7
- Probes:
- 3mm Triple-resonance Inverse (TCI) cryoprobe with Z-Gradients
- 3mm BBI room-temperature probe with Z-Gradients (15N to 31P)
- 3.2mm HX low-gamma solids probe (29Si to 13C)
- 1.9mm HX high-gamma solids probe (13C to 31P)
- 1.3mm HCN fast MAS probe (up to 67 kHz)
- 0.7mm HCN ultra-fast MAS probe (up to 111 kHz)
- Features: Temperature controlled SampleCase (up to 24 samples), Nitrogen Liquefier
- Location: CBEC 092
Training
Expert NMR training and consultation on experiment design, data collection, and analysis.